2
0
2005
sch
gre
0
journal
Original
Schmelzer, J.[Juergen]
Grenner, A.[Andreas]
Matusche, J.[Jan]
Brettschneider, G.[Gabi]
Anderson, J.[Joerg]
Niederbroeker, H.[Heike]
J. Chem. Eng. Data
2005
2005-08-19
Activity Coefficients at Infinite Dilution and Excess Molar Volumes in Binary Mixtures Containing Normal Alkanes (Nonane, Decane, Undecane, or Dodecane) and Cresols (2-Methylphenol or 3-Methylphenol)
The differential ebulliometry method was used to measure activity coefficients at infinite dilution for cresols (2-methylphenol or 3-mehtylphenol) with nonane, decane, or undecane a in a range of temperature from (373 to 433) K. Temperature-dependent parameters were determined for the UNIQUAC model. Densities of binary mixtures of systems containing 2-cresol + nonane or decane or undecane and 3-cresol + nonane or undecane or dodecane have been measured at 308.15 K under atmospheric pressure. With these data, excess molar volumes (VE) have been calculated. The excess molar volumes were fitted to the Redlich-Kister polynomial equation.
Activity Coefficients at Infinite Dilution and Excess Molar Volumes in Binary Mixtures Containing Normal Alkanes (Nonane
Decane
Undecane
or Dodecane) and Cresols (2-Methylphenol or 3-Methylphenol)
50
1250-1254
1
2-methylphenol
C7H8O
1
Commercial source
1
98
2
Stated by supplier
2
Dried with chemical reagent
Fractional distillation
2
99.1
3
Gas chromatography
2
3-methylphenol
C7H8O
1
Commercial source
1
99
2
Stated by supplier
2
Dried with chemical reagent
Fractional distillation
2
99.9
3
Gas chromatography
3
nonane
C9H20
1
Commercial source
1
99
2
Stated by supplier
2
Fractional distillation
Molecular sieve treatment
2
99.9
3
Gas chromatography
4
decane
C10H22
1
Commercial source
1
98
2
Stated by supplier
2
Fractional distillation
Molecular sieve treatment
2
99.4
3
Gas chromatography
5
undecane
C11H24
1
Commercial source
1
98
2
Stated by supplier
2
Fractional distillation
Molecular sieve treatment
2
99.9
3
Gas chromatography
6
dodecane
C12H26
1
Commercial source
1
98
2
Stated by supplier
2
Fractional distillation
Molecular sieve treatment
2
99.7
3
Gas chromatography
1
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Refractive index (Na D-line)
Standard Abbe refractometry
Liquid
Direct value, X
Liquid
Pressure, kPa
101.325
6
1
Temperature, K
1
308.15
5
1
1.5386
5
1
1
Principal objective of the work
JCE
JCE
8/18/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
1
Pressure, kPa
2
Temperature, K
1
101.3
4
2
308.15
5
1
1032.73
6
2
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Refractive index (Na D-line)
Standard Abbe refractometry
Liquid
Direct value, X
Liquid
Pressure, kPa
101.325
6
1
Temperature, K
1
293.15
5
1
1.5401
5
2
1
Principal objective of the work
JCE
JCE
8/18/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
1
Pressure, kPa
2
Temperature, K
1
101.3
4
2
308.15
5
1
1022.02
6
3
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Refractive index (Na D-line)
Standard Abbe refractometry
Liquid
Direct value, X
Liquid
Pressure, kPa
101.325
6
1
Temperature, K
1
293.15
5
1
1.4058
5
3
1
Principal objective of the work
JCE
JCE
8/18/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
1
Pressure, kPa
2
Temperature, K
1
101.3
4
2
308.15
5
1
707.41
5
4
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Refractive index (Na D-line)
Standard Abbe refractometry
Liquid
Direct value, X
Liquid
Pressure, kPa
101.325
6
1
Temperature, K
1
308.15
5
1
1.4055
5
4
1
Principal objective of the work
JCE
JCE
8/18/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
1
Pressure, kPa
2
Temperature, K
1
101.3
4
2
308.15
5
1
720.24
5
5
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Refractive index (Na D-line)
Standard Abbe refractometry
Liquid
Direct value, X
Liquid
Pressure, kPa
101.325
6
1
Temperature, K
1
293.15
5
1
1.4164
5
5
1
Principal objective of the work
JCE
JCE
8/18/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
1
Pressure, kPa
2
Temperature, K
1
101.3
4
2
308.15
5
1
729.13
5
6
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Refractive index (Na D-line)
Standard Abbe refractometry
Liquid
Direct value, X
Liquid
Pressure, kPa
101.325
6
1
Temperature, K
1
293.15
5
1
1.421
5
6
1
Principal objective of the work
JCE
JCE
8/18/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
1
Pressure, kPa
2
Temperature, K
1
101.3
4
2
308.15
5
1
738.63
5
1
1
3
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Activity coefficient
Differential ebulliometry
1
Liquid
Direct value, X
Pure compound
1
Author
Liquid
Pressure, kPa
101.3
4
Mole fraction
1
Liquid
0
0
1
Temperature, K
1
373.15
5
1
5.84
3
1
.4088
1
393.15
5
1
4.58
3
1
.3206
1
413.15
5
1
3.8
2
1
.266
1
1
3
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
Pressure, kPa
101.3
4
Temperature, K
308.15
5
1
Mole fraction
1
Liquid
1
0
0
1
707.41
5
1
.0661
3
1
719.58
5
1
.0684
3
1
720.02
5
1
.1489
4
1
736.5
5
1
.2085
4
1
749.6
5
1
.2703
4
1
764.08
5
1
.3994
4
1
797.32
5
1
.4008
4
1
797.69
5
1
.4688
4
1
817.04
5
1
.5237
4
1
833.66
5
1
.5941
4
1
856.51
5
1
.6631
4
1
880.76
5
1
.7323
4
1
906.98
5
1
.8106
4
1
939.53
5
1
.8674
4
1
965.12
5
1
.9285
4
1
994.76
5
1
1
5
1
1032.73
6
1
1
4
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Activity coefficient
Differential ebulliometry
1
Liquid
Direct value, X
Pure compound
1
Author
Liquid
Pressure, kPa
101.3
4
Mole fraction
1
Liquid
0
0
1
Temperature, K
1
393.15
5
1
4.15
3
1
.2905
1
413.15
5
1
3.49
3
1
.2443
1
433.15
5
1
3.04
3
1
.2128
1
1
4
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
Pressure, kPa
101.3
4
Temperature, K
308.15
5
1
Mole fraction
1
Liquid
1
0
0
1
720.24
5
1
.0637
3
1
730.49
5
1
.0908
3
1
735.2
5
1
.162
4
1
748.33
5
1
.2086
4
1
757.57
5
1
.272
4
1
770.9
5
1
.3186
4
1
781.32
5
1
.4014
4
1
801.21
5
1
.4707
4
1
819.47
5
1
.529
4
1
836.06
5
1
.6014
4
1
858.4
5
1
.6596
4
1
878.02
5
1
.7379
4
1
906.95
5
1
.7876
4
1
927.04
5
1
.8714
4
1
964.58
5
1
.9348
4
1
996.28
5
1
.9617
4
1
1010.78
6
1
1
5
1
1032.73
6
1
1
5
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Activity coefficient
Differential ebulliometry
1
Liquid
Direct value, X
Pure compound
1
Author
Liquid
Pressure, kPa
101.3
4
Mole fraction
1
Liquid
0
0
1
Temperature, K
1
393.15
5
1
4.47
3
1
.3129
1
413.15
5
1
3.77
3
1
.2639
1
433.15
5
1
2.85
3
1
.1995
1
1
5
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
Pressure, kPa
101.3
4
Temperature, K
308.15
5
1
Mole fraction
1
Liquid
1
0
0
1
729.13
5
1
.0367
3
1
734.21
5
1
.0684
3
1
738.92
5
1
.0746
3
1
739.92
5
1
.1306
4
1
748.8
5
1
.2094
4
1
762.7
5
1
.2809
4
1
776.41
5
1
.3636
4
1
794.01
5
1
.4749
4
1
820.79
5
1
.5311
4
1
835.93
5
1
.5989
4
1
855.95
5
1
.6593
4
1
875.61
5
1
.7261
4
1
899.41
5
1
.8065
4
1
931.92
5
1
.8662
4
1
959.18
5
1
.9476
4
1
1001.43
6
1
1
5
1
1032.73
6
2
1
3
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Activity coefficient
Differential ebulliometry
2
Liquid
Direct value, X
Pure compound
1
Author
Liquid
Pressure, kPa
101.3
4
Mole fraction
2
Liquid
0
0
1
Temperature, K
1
373.15
5
1
9.21
3
1
.6447
1
393.15
5
1
7.06
3
1
.4942
1
413.15
5
1
5.96
3
1
.4172
2
1
3
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
Pressure, kPa
101.3
4
Temperature, K
308.15
5
1
Mole fraction
2
Liquid
1
0
0
1
707.41
5
1
.1021
4
1
726.54
5
1
.1998
4
1
747.24
5
1
.302
4
1
770.94
5
1
.4021
4
1
796.76
5
1
.5
4
1
825
5
1
.7
4
1
892.22
5
1
.9
4
1
974.43
5
1
1
5
1
1022.02
6
2
1
4
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Activity coefficient
Differential ebulliometry
2
Liquid
Direct value, X
Pure compound
1
Author
Liquid
Pressure, kPa
101.3
4
Mole fraction
2
Liquid
0
0
1
Temperature, K
1
373.15
5
1
7.79
3
1
.5453
1
403.15
5
1
5.37
3
1
.3759
1
433.15
5
1
4.26
3
1
.2982
2
1
5
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Activity coefficient
Differential ebulliometry
2
Liquid
Direct value, X
Pure compound
1
Author
Liquid
Pressure, kPa
101.3
4
Mole fraction
2
Liquid
0
0
1
Temperature, K
1
393.15
5
1
6.25
3
1
.4375
1
413.15
5
1
4.9
3
1
.343
1
433.15
5
1
3.93
3
1
.2751
2
1
5
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
Pressure, kPa
101.3
4
Temperature, K
308.15
5
1
Mole fraction
2
Liquid
1
0
0
1
729.13
5
1
.1287
4
1
748.52
5
1
.1853
4
1
758.11
5
1
.3395
4
1
787.84
5
1
.389
4
1
798.63
5
1
.5024
4
1
826.11
5
1
.6023
4
1
854.21
5
1
.6949
4
1
884.19
5
1
.8
4
1
923.73
5
1
.9
4
1
968.61
5
1
1
5
1
1022.02
6
2
1
6
1
Principal objective of the work
NEO
JCE
7/19/2005
1
Mass density, kg/m3
Vibrating tube method
Liquid
Direct value, X
Liquid
Pressure, kPa
101.3
4
Temperature, K
308.15
5
1
Mole fraction
2
Liquid
1
0
0
1
738.63
5
1
.1325
4
1
756.67
5
1
.2055
4
1
767.97
5
1
.3009
4
1
784.51
5
1
.4009
4
1
804.35
5
1
.6976
4
1
883.71
5
1
.7987
4
1
921.29
5
1
.895
4
1
963.9
5
1
1
5
1
1022.02
6